Crystal Structure of 3-acetoxy-2-methyl-N-(4-nitrophenyl)benzamide

KANSIZ, SEVGİ; çakmak, Şükriye; Dege, Necmi; Meral, Güngör; Kütük, Halil

doi:10.2116/xraystruct.34.17

Crystal Structure of 3-acetoxy-2-methyl-N-(4-nitrophenyl)benzamide

KANSIZ S., çakmak Ş., Dege N., Meral G., Kütük H.

X-ray Structure Analysis Online, cilt.34, sa.5, ss.17-18, 2018 (Scopus)

Yayın Türü: Makale / Tam Makale
Cilt numarası: 34 Sayı: 5
Basım Tarihi: 2018
Doi Numarası: 10.2116/xraystruct.34.17
Dergi Adı: X-ray Structure Analysis Online
Derginin Tarandığı İndeksler: Scopus
Sayfa Sayıları: ss.17-18
Açık Arşiv Koleksiyonu: AVESİS Açık Erişim Koleksiyonu
Samsun Üniversitesi Adresli: Hayır

Özet

The structure of 3-acetoxy-2-methyl-N-(4-nitrophenyl)benzamide was determined by X-ray crystallography. The compound crystallized in a monoclinic system and it was characterized in the space group P21/c with cell parameters a = 5.8658(3), b = 17.1661(10), c = 15.1938(7)Å, β = 103.182(4)°s, Z = 4, V = 1489.60(14)Å3. The R1 [I > 2σ(I)] and wR2 (all data) values are 0.046 and 0.093, respectively, for all 2932 independent reflections. Intramolecular C3-H3···O3 and intermolecular N2-H2···O1, C5-H5···O1 interactions were observed in the crystal lattice.